TA Instruments

AR1711-0001f

04/09/2012 17:05:52

Sample name	ASW 10 mm from base, 60 mm to top, disk 9 PMMA fouled AND CLEANED
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1711
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 17:05:52

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

-36.46	5.899	-6.180	1.0080	22.4	412.5	2.2632	10000	0.1012	11.85	2.8290	282.90	3.383E-3	0.0	1.0	61.008	-111.85	4.719
0.7684	12.70	0.06049	2.0080	22.4	398.4	13.7488	10000	0.09779	2.469	17.186	1718.6	3.384E-3	0.0	1.0	62.008	2.3575	10.16
1.499	19.55	0.07667	3.0080	22.4	405.9	27.3986	10000	0.09962	1.062	34.248	3424.8	3.384E-3	0.1	1.1	63.008	4.5989	15.64
2.049	23.20	0.08832	3.9920	22.4	400.1	41.3245	10000	0.09820	0.7436	51.656	5165.6	3.384E-3	0.1	1.1	63.992	6.2850	18.56
3.324	30.96	0.1074	4.9920	22.4	398.4	68.0334	10000	0.09779	0.4157	85.042	8504.2	3.384E-3	0.1	1.1	64.992	10.197	24.77
5.093	39.57	0.1287	6.0120	22.4	403.4	107.1500	10000	0.09901	0.2576	133.94	13394	3.384E-3	0.1	1.1	66.012	15.625	31.66
5.899	42.62	0.1384	7.0080	22.4	409.2	126.7790	10000	0.1004	0.2253	158.47	15847	3.384E-3	0.1	1.1	67.008	18.097	34.09
7.499	49.20	0.1524	8.0080	22.4	397.6	165.9410	10000	0.09759	0.1642	207.43	20743	3.384E-3	0.1	1.1	68.008	23.007	39.36
9.717	57.60	0.1687	9.0120	22.4	412.5	223.7770	10000	0.1012	0.1243	279.72	27972	3.384E-3	0.2	1.2	69.012	29.810	46.08
11.80	63.75	0.1852	10.008	22.4	401.8	275.2230	10000	0.09860	0.09886	344.03	34403	3.384E-3	0.2	1.2	70.008	36.216	51.00
13.76	69.70	0.1975	11.008	22.4	389.4	326.9040	10000	0.09556	0.08014	408.63	40863	3.384E-3	0.2	1.2	71.008	42.226	55.76
15.63	75.17	0.2080	12.008	22.4	396.8	377.6240	10000	0.09739	0.07023	472.03	47203	3.384E-3	0.2	1.2	72.008	47.957	60.13
17.34	80.56	0.2153	13.008	22.4	393.5	435.5370	10000	0.09658	0.06064	544.42	54442	3.384E-3	0.2	1.2	73.008	53.200	64.44
19.53	86.47	0.2259	14.008	22.4	393.5	499.0660	10000	0.09658	0.05263	623.83	62383	3.384E-3	0.2	1.2	74.008	59.922	69.18
22.50	94.64	0.2377	15.008	22.4	398.4	594.6470	10000	0.09779	0.04448	743.31	74331	3.384E-3	0.3	1.3	75.008	69.030	75.71
24.87	99.95	0.2488	16.004	22.4	390.2	664.7560	10000	0.09576	0.03906	830.95	83095	3.384E-3	0.3	1.3	76.004	76.291	79.96
26.94	105.7	0.2549	17.004	22.4	387.7	741.1010	10000	0.09516	0.03470	926.38	92638	3.383E-3	0.3	1.3	77.004	82.663	84.56
30.24	113.8	0.2658	18.004	22.4	393.5	855.5570	10000	0.09658	0.03040	1069.4	1.0694E5	3.383E-3	0.3	1.3	78.004	92.773	91.01
32.45	118.8	0.2731	19.008	22.4	374.5	931.6290	10000	0.09191	0.02652	1164.5	1.1645E5	3.383E-3	0.3	1.3	79.008	99.557	95.06
34.98	124.3	0.2814	20.008	22.4	375.3	1020.5700	10000	0.09211	0.02430	1275.7	1.2757E5	3.383E-3	0.3	1.3	80.008	107.30	99.42
38.36	132.3	0.2899	21.008	22.4	370.3	1154.4200	10000	0.09090	0.02115	1443.0	1.4430E5	3.384E-3	0.4	1.4	81.008	117.68	105.8
40.91	137.4	0.2977	22.008	22.4	378.6	1244.3101	10000	0.09292	0.02005	1555.4	1.5554E5	3.383E-3	0.4	1.4	82.008	125.50	109.9
43.25	142.8	0.3028	23.004	22.4	372.8	1343.9700	10000	0.09150	0.01828	1680.0	1.6800E5	3.383E-3	0.4	1.4	83.004	132.68	114.3
47.37	150.8	0.3141	24.008	22.4	363.7	1496.1000	10000	0.08927	0.01599	1870.1	1.8701E5	3.383E-3	0.4	1.4	84.008	145.33	120.7
49.65	155.9	0.3184	25.008	22.4	358.8	1597.7000	10000	0.08805	0.01475	1997.1	1.9971E5	3.383E-3	0.4	1.4	85.008	152.33	124.8
53.00	161.3	0.3285	26.008	22.4	351.3	1711.5800	10000	0.08623	0.01350	2139.5	2.1395E5	3.383E-3	0.4	1.4	86.008	162.60	129.1
57.34	169.3	0.3386	27.008	22.4	352.2	1882.5200	10000	0.08643	0.01228	2353.2	2.3532E5	3.384E-3	0.5	1.5	87.008	175.92	135.5
59.47	174.5	0.3409	28.012	22.4	355.5	1996.3900	10000	0.08724	0.01168	2495.5	2.4955E5	3.384E-3	0.5	1.5	88.012	182.46	139.6
62.55	179.6	0.3483	29.008	22.4	352.2	2116.5300	10000	0.08643	0.01092	2645.7	2.6457E5	3.384E-3	0.5	1.5	89.008	191.89	143.7
66.85	187.6	0.3564	30.008	22.4	353.8	2306.3401	10000	0.08684	0.01006	2882.9	2.8829E5	3.384E-3	0.5	1.5	90.008	205.10	150.1
70.67	192.7	0.3667	31.008	22.4	335.6	2433.7700	10000	0.08237	9.037E-3	3042.2	3.0422E5	3.384E-3	0.5	1.5	91.008	216.82	154.2
73.32	197.8	0.3706	32.008	22.4	346.4	2636.5500	10000	0.08501	8.849E-3	3295.7	3.2957E5	3.384E-3	0.5	1.5	92.008	224.96	158.3
78.15	205.8	0.3796	33.032	22.4	338.1	2774.1001	10000	0.08298	7.980E-3	3467.6	3.4676E5	3.384E-3	0.6	1.6	93.032	239.75	164.7
81.37	211.0	0.3857	34.008	22.4	330.7	2913.3601	10000	0.08116	7.427E-3	3641.7	3.6417E5	3.384E-3	0.6	1.6	94.008	249.65	168.8
85.60	218.6	0.3916	35.008	22.4	341.4	3128.1101	10000	0.08379	7.143E-3	3910.1	3.9101E5	3.384E-3	0.6	1.6	95.008	262.62	174.9
89.39	223.9	0.3992	36.008	22.4	310.0	3279.7800	10000	0.07608	6.183E-3	4099.7	4.0997E5	3.384E-3	0.6	1.6	96.008	274.26	179.1
92.93	229.1	0.4057	36.992	22.4	310.8	3431.3899	10000	0.07629	5.922E-3	4289.2	4.2892E5	3.384E-3	0.6	1.6	96.992	285.12	183.3
98.19	236.6	0.4149	38.004	22.4	307.5	3658.5901	10000	0.07548	5.491E-3	4573.2	4.5732E5	3.384E-3	0.6	1.6	98.004	301.23	189.3
101.1	241.9	0.4180	39.008	22.4	303.4	3827.6399	10000	0.07446	5.187E-3	4784.6	4.7846E5	3.384E-3	0.7	1.7	99.008	310.19	193.5
105.9	249.6	0.4241	39.992	22.4	289.3	4069.0000	10000	0.07101	4.644E-3	5086.3	5.0863E5	3.384E-3	0.7	1.7	99.992	324.76	199.7
109.7	254.6	0.4306	40.992	22.4	277.8	4233.0698	10000	0.06817	4.284E-3	5291.3	5.2913E5	3.384E-3	0.7	1.7	100.992	336.42	203.7
113.9	262.5	0.4339	42.012	22.4	286.0	4499.9902	10000	0.07020	4.152E-3	5625.0	5.6250E5	3.383E-3	0.7	1.7	102.012	349.43	210.0
119.2	267.6	0.4453	43.004	22.4	246.3	4675.0098	10000	0.06046	3.439E-3	5843.8	5.8438E5	3.383E-3	0.7	1.7	103.004	365.61	214.1
122.7	272.7	0.4499	44.012	22.4	257.9	4851.7500	10000	0.06330	3.469E-3	6064.7	6.0647E5	3.383E-3	0.7	1.7	104.012	376.35	218.2
128.7	280.4	0.4590	45.008	22.4	258.7	5129.4600	10000	0.06350	3.292E-3	6411.8	6.4118E5	3.383E-3	0.8	1.8	105.008	394.82	224.3
132.6	285.5	0.4645	46.008	22.4	250.5	5318.6899	10000	0.06148	3.072E-3	6648.4	6.6484E5	3.383E-3	0.8	1.8	106.008	406.87	228.4
137.6	293.1	0.4693	47.008	22.4	263.7	5602.6699	10000	0.06472	3.069E-3	7003.3	7.0033E5	3.383E-3	0.8	1.8	107.008	422.02	234.5
141.8	298.2	0.4754	48.008	22.4	256.3	5798.3101	10000	0.06290	2.883E-3	7247.9	7.2479E5	3.384E-3	0.8	1.8	108.008	434.89	238.5
144.7	303.4	0.4771	49.008	22.4	260.4	6002.1699	10000	0.06391	2.830E-3	7502.7	7.5027E5	3.384E-3	0.8	1.8	109.008	444.01	242.7
152.7	311.0	0.4911	50.008	22.4	238.1	6302.7598	10000	0.05843	2.462E-3	7878.5	7.8785E5	3.384E-3	0.8	1.8	110.008	468.54	248.8
158.0	316.0	0.4999	51.008	22.4	244.7	6511.0801	10000	0.06006	2.450E-3	8138.9	8.1389E5	3.384E-3	0.9	1.9	111.008	484.64	252.8
161.6	323.8	0.4991	52.008	22.4	227.3	6833.4399	10000	0.05579	2.168E-3	8541.8	8.5418E5	3.384E-3	0.9	1.9	112.008	495.86	259.0
164.6	328.9	0.5006	53.008	22.4	218.2	7048.0801	10000	0.05356	2.018E-3	8810.1	8.8101E5	3.384E-3	0.9	1.9	113.008	505.11	263.1
172.4	336.4	0.5126	54.008	22.4	205.8	7376.7598	10000	0.05052	1.819E-3	9221.0	9.2210E5	3.383E-3	0.9	1.9	114.008	529.04	269.1
177.7	341.6	0.5202	55.008	22.4	214.1	7601.9302	10000	0.05255	1.835E-3	9502.4	9.5024E5	3.383E-3	0.9	1.9	115.008	545.21	273.3
185.1	346.7	0.5340	56.008	22.4	195.9	7828.7998	10000	0.04809	1.630E-3	9786.0	9.7860E5	3.384E-3	0.9	1.9	116.008	568.02	277.4
188.2	354.2	0.5314	57.008	22.4	191.0	8169.3599	10000	0.04687	1.522E-3	10212	1.0212E6	3.384E-3	1.0	2.0	117.008	577.47	283.4
192.4	359.4	0.5353	58.008	22.4	205.0	8408.7500	10000	0.05032	1.588E-3	10511	1.0511E6	3.384E-3	1.0	2.0	118.008	590.20	287.5
199.3	367.0	0.5430	59.008	22.4	205.8	8768.1797	10000	0.05052	1.528E-3	10960	1.0960E6	3.384E-3	1.0	2.0	119.008	611.41	293.6
202.5	372.0	0.5444	60.008	22.4	207.5	9007.6504	10000	0.05093	1.499E-3	11260	1.1260E6	3.384E-3	1.0	2.0	120.008	621.30	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

207.4	375.0	0.5532	1.0080	22.4	190.1	293.4260	10000	0.04666	1.352E-3	366.78	36678	3.384E-3	0.0	2.0	122.008	636.41	300.0
204.4	375.0	0.5450	2.0120	22.4	185.2	544.5070	10000	0.04545	1.317E-3	680.63	68063	3.383E-3	0.0	2.1	123.012	626.97	300.0
207.8	375.0	0.5540	3.0240	22.4	181.9	934.4180	10000	0.04464	1.293E-3	1168.0	1.1680E5	3.384E-3	0.1	2.1	124.024	637.42	300.0
205.8	375.0	0.5488	4.0240	22.4	219.1	1174.0300	10000	0.05377	1.558E-3	1467.5	1.4675E5	3.384E-3	0.1	2.1	125.024	631.35	300.0
207.8	375.0	0.5542	5.1200	22.4	181.0	1549.9500	10000	0.04443	1.287E-3	1937.4	1.9374E5	3.384E-3	0.1	2.1	126.120	637.59	300.0
207.9	375.0	0.5543	6.0120	22.4	153.8	1801.3000	10000	0.03774	1.093E-3	2251.6	2.2516E5	3.384E-3	0.1	2.1	127.012	637.69	300.0
207.9	375.0	0.5544	7.0080	22.4	176.9	2053.9900	10000	0.04342	1.258E-3	2567.5	2.5675E5	3.383E-3	0.1	2.1	128.008	637.86	300.0
207.8	375.0	0.5543	8.0080	22.4	185.2	2431.8701	10000	0.04545	1.317E-3	3039.8	3.0398E5	3.384E-3	0.1	2.2	129.008	637.67	300.0
206.8	375.0	0.5516	9.0080	22.4	186.8	2681.1201	10000	0.04585	1.329E-3	3351.4	3.3514E5	3.384E-3	0.2	2.2	130.008	634.57	300.0
207.8	375.0	0.5540	10.024	22.4	190.1	2932.1399	10000	0.04666	1.352E-3	3665.2	3.6652E5	3.383E-3	0.2	2.2	131.024	637.43	300.0
205.9	375.0	0.5491	11.020	22.4	190.1	3311.3401	10000	0.04666	1.352E-3	4139.2	4.1392E5	3.383E-3	0.2	2.2	132.020	631.73	300.0
208.0	375.0	0.5546	12.008	22.4	157.9	3560.4399	10000	0.03875	1.123E-3	4450.6	4.4506E5	3.383E-3	0.2	2.2	133.008	638.02	300.0
207.5	375.0	0.5533	13.024	22.4	176.9	3940.6001	10000	0.04342	1.258E-3	4925.8	4.9258E5	3.383E-3	0.2	2.2	134.024	636.61	300.0
207.4	375.0	0.5530	14.024	22.4	167.0	4188.7598	10000	0.04098	1.187E-3	5236.0	5.2360E5	3.383E-3	0.2	2.3	135.024	636.20	300.0
206.8	375.0	0.5514	15.008	22.4	196.7	4440.2402	10000	0.04829	1.399E-3	5550.3	5.5503E5	3.383E-3	0.3	2.3	136.008	634.33	300.0
204.7	375.0	0.5460	16.008	22.4	174.4	4817.2700	10000	0.04281	1.240E-3	6021.6	6.0216E5	3.383E-3	0.3	2.3	137.008	628.15	300.0
209.4	375.0	0.5583	17.020	22.4	167.8	5070.1001	10000	0.04119	1.193E-3	6337.6	6.3376E5	3.383E-3	0.3	2.3	138.020	642.31	300.0
208.2	375.0	0.5553	18.008	22.4	144.7	5319.9702	10000	0.03551	1.029E-3	6650.0	6.6500E5	3.383E-3	0.3	2.3	139.008	638.88	300.0
205.8	375.0	0.5489	19.020	22.4	176.9	5699.2300	10000	0.04342	1.258E-3	7124.0	7.1240E5	3.383E-3	0.3	2.3	140.020	631.52	300.0
206.5	375.0	0.5505	20.008	22.4	171.9	5948.1602	10000	0.04220	1.223E-3	7435.2	7.4352E5	3.383E-3	0.3	2.4	141.008	633.39	300.0
205.6	375.0	0.5482	21.024	22.4	185.2	6325.0298	10000	0.04545	1.317E-3	7906.3	7.9063E5	3.384E-3	0.4	2.4	142.024	630.74	300.0
206.7	375.0	0.5512	22.008	22.4	166.2	6576.5098	10000	0.04078	1.182E-3	8220.6	8.2206E5	3.384E-3	0.4	2.4	143.008	634.17	300.0
207.0	375.0	0.5521	23.008	22.4	167.8	6827.7202	10000	0.04119	1.193E-3	8534.7	8.5347E5	3.384E-3	0.4	2.4	144.008	635.20	300.0
208.0	375.0	0.5547	24.008	22.4	167.8	7204.9102	10000	0.04119	1.193E-3	9006.1	9.0061E5	3.384E-3	0.4	2.4	145.008	638.16	300.0
207.6	375.0	0.5537	25.012	22.4	175.3	7456.0801	10000	0.04301	1.246E-3	9320.1	9.3201E5	3.383E-3	0.4	2.4	146.012	636.99	300.0
205.7	375.0	0.5484	26.008	22.4	205.0	7835.2100	10000	0.05032	1.458E-3	9794.0	9.7940E5	3.384E-3	0.4	2.5	147.008	630.95	300.0
205.6	375.0	0.5482	27.008	22.4	176.1	8086.2300	10000	0.04322	1.252E-3	10108	1.0108E6	3.384E-3	0.5	2.5	148.008	630.71	300.0
205.8	375.0	0.5487	28.008	22.4	190.1	8338.0400	10000	0.04666	1.352E-3	10423	1.0423E6	3.384E-3	0.5	2.5	149.008	631.28	300.0
207.4	375.0	0.5531	29.004	22.4	186.8	8714.2197	10000	0.04585	1.329E-3	10893	1.0893E6	3.384E-3	0.5	2.5	150.004	636.31	300.0
207.3	375.0	0.5528	30.004	22.4	185.2	8976.2598	10000	0.04545	1.317E-3	11220	1.1220E6	3.384E-3	0.5	2.5	151.004	636.04	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

205.3	370.2	0.5545	0.99200	22.4	176.9	311.9530	10000	0.04342	1.291E-3	389.94	38994	3.384E-3	0.0	2.5	151.992	629.85	296.2
196.8	365.2	0.5388	2.0080	22.4	219.1	550.0190	10000	0.05377	1.643E-3	687.52	68752	3.384E-3	0.0	2.6	153.008	603.69	292.2
192.6	360.1	0.5348	3.0080	22.4	205.0	910.0650	10000	0.05032	1.581E-3	1137.6	1.1376E5	3.384E-3	0.1	2.6	154.008	590.86	288.1
189.4	352.4	0.5374	4.0120	22.4	200.0	1145.0900	10000	0.04910	1.611E-3	1431.4	1.4314E5	3.384E-3	0.1	2.6	155.012	580.97	281.9
185.3	347.3	0.5336	4.9920	22.4	174.4	1373.5500	10000	0.04281	1.446E-3	1716.9	1.7169E5	3.384E-3	0.1	2.6	155.992	568.60	277.9
178.2	339.7	0.5245	6.0080	22.4	221.5	1708.4700	10000	0.05437	1.920E-3	2135.6	2.1356E5	3.384E-3	0.1	2.6	157.008	546.61	271.8
173.2	334.5	0.5177	6.9920	22.4	190.1	1933.6400	10000	0.04666	1.699E-3	2417.1	2.4171E5	3.384E-3	0.1	2.6	157.992	531.36	267.6
168.4	327.0	0.5151	7.9960	22.4	226.5	2254.1899	10000	0.05559	2.118E-3	2817.7	2.8177E5	3.383E-3	0.1	2.6	158.996	516.75	261.6
163.9	321.9	0.5093	9.0120	22.4	228.2	2465.9299	10000	0.05600	2.202E-3	3082.4	3.0824E5	3.384E-3	0.2	2.7	160.012	502.98	257.5
159.1	316.8	0.5022	9.9920	22.4	220.7	2678.6699	10000	0.05417	2.200E-3	3348.3	3.3483E5	3.384E-3	0.2	2.7	160.992	488.08	253.4
152.9	309.1	0.4946	10.992	22.4	223.2	2985.3000	10000	0.05478	2.336E-3	3731.6	3.7316E5	3.383E-3	0.2	2.7	161.992	469.10	247.3
147.9	304.1	0.4864	11.992	22.4	217.4	3187.6699	10000	0.05336	2.352E-3	3984.6	3.9846E5	3.383E-3	0.2	2.7	162.992	453.76	243.2
139.8	296.3	0.4719	12.992	22.4	256.3	3487.3799	10000	0.06290	2.919E-3	4359.2	4.3592E5	3.384E-3	0.2	2.7	163.992	429.01	237.1
136.3	291.1	0.4683	13.992	22.4	262.9	3683.1299	10000	0.06452	3.101E-3	4603.9	4.6039E5	3.384E-3	0.2	2.7	164.992	418.29	232.9
129.2	283.6	0.4558	14.992	22.4	275.3	3962.7500	10000	0.06756	3.424E-3	4953.4	4.9534E5	3.384E-3	0.2	2.8	165.992	396.47	226.8
128.3	278.4	0.4609	16.008	22.4	249.6	4149.3799	10000	0.06127	3.221E-3	5186.7	5.1867E5	3.384E-3	0.3	2.8	167.008	393.61	222.7
123.9	273.2	0.4536	17.000	22.4	255.4	4330.6802	10000	0.06269	3.422E-3	5413.4	5.4134E5	3.384E-3	0.3	2.8	168.000	380.19	218.6
118.5	265.7	0.4462	18.008	22.4	279.4	4593.6099	10000	0.06858	3.959E-3	5742.0	5.7420E5	3.383E-3	0.3	2.8	169.008	363.63	212.5
112.7	260.5	0.4327	19.012	22.4	286.8	4768.7798	10000	0.07040	4.226E-3	5961.0	5.9610E5	3.384E-3	0.3	2.8	170.012	345.80	208.4
110.3	252.7	0.4366	19.992	22.4	291.8	5024.9199	10000	0.07162	4.570E-3	6281.2	6.2812E5	3.383E-3	0.3	2.8	170.992	338.46	202.1
105.8	247.7	0.4274	21.012	22.4	300.1	5188.7598	10000	0.07365	4.892E-3	6486.0	6.4860E5	3.384E-3	0.4	2.9	172.012	324.71	198.1
101.4	242.5	0.4181	22.008	22.4	290.2	5350.1201	10000	0.07121	4.933E-3	6687.7	6.6877E5	3.384E-3	0.4	2.9	173.008	311.13	194.0
96.94	234.6	0.4132	23.008	22.4	295.1	5593.8999	10000	0.07243	5.361E-3	6992.4	6.9924E5	3.384E-3	0.4	2.9	174.008	297.41	187.7
93.13	229.5	0.4058	23.992	22.4	315.0	5744.7500	10000	0.07730	5.978E-3	7180.9	7.1809E5	3.384E-3	0.4	2.9	174.992	285.72	183.6
88.41	221.8	0.3986	24.992	22.4	315.0	5969.6401	10000	0.07730	6.401E-3	7462.1	7.4621E5	3.384E-3	0.4	2.9	175.992	271.24	177.4
84.49	216.5	0.3902	25.992	22.4	328.2	6118.9399	10000	0.08055	7.000E-3	7648.7	7.6487E5	3.383E-3	0.4	2.9	176.992	259.22	173.2
80.97	211.4	0.3829	26.992	22.4	305.0	6257.8701	10000	0.07487	6.823E-3	7822.3	7.8223E5	3.384E-3	0.4	3.0	177.992	248.41	169.1
76.34	203.8	0.3747	27.992	22.4	314.1	6462.3101	10000	0.07710	7.566E-3	8077.9	8.0779E5	3.384E-3	0.5	3.0	178.992	234.21	163.0
73.34	198.5	0.3695	28.992	22.4	311.6	6600.5098	10000	0.07649	7.912E-3	8250.6	8.2506E5	3.383E-3	0.5	3.0	179.992	225.00	158.8
68.81	190.6	0.3609	30.008	22.4	334.0	6793.3799	10000	0.08197	9.189E-3	8491.7	8.4917E5	3.384E-3	0.5	3.0	181.008	211.10	152.5
65.56	185.5	0.3534	31.008	22.4	324.0	6918.7202	10000	0.07953	9.416E-3	8648.4	8.6484E5	3.384E-3	0.5	3.0	182.008	201.12	148.4
62.94	180.2	0.3492	31.984	22.4	336.4	7044.8901	10000	0.08258	0.01036	8806.1	8.8061E5	3.384E-3	0.5	3.0	182.984	193.09	144.2
57.75	172.4	0.3349	32.992	22.4	356.3	7218.5298	10000	0.08745	0.01198	9023.2	9.0232E5	3.384E-3	0.5	3.1	183.992	177.17	137.9
55.26	167.3	0.3303	33.992	22.4	351.3	7330.0098	10000	0.08623	0.01255	9162.5	9.1625E5	3.384E-3	0.6	3.1	184.992	169.52	133.9
52.33	162.0	0.3229	34.992	22.4	360.4	7443.2900	10000	0.08846	0.01373	9304.1	9.3041E5	3.384E-3	0.6	3.1	185.992	160.55	129.6
47.96	154.0	0.3115	36.004	22.4	366.2	7604.3599	10000	0.08988	0.01545	9505.5	9.5055E5	3.384E-3	0.6	3.1	187.004	147.13	123.2
45.57	148.9	0.3061	36.992	22.4	348.8	7704.0898	10000	0.08562	0.01574	9630.1	9.6301E5	3.384E-3	0.6	3.1	187.992	139.80	119.1
43.27	143.6	0.3014	37.988	22.4	352.2	7803.7202	10000	0.08643	0.01708	9754.7	9.7547E5	3.384E-3	0.6	3.1	188.988	132.75	114.9
39.26	135.5	0.2898	38.992	22.4	362.1	7946.9600	10000	0.08887	0.01973	9933.7	9.9337E5	3.383E-3	0.6	3.2	189.992	120.44	108.4
37.22	130.4	0.2855	40.004	22.4	365.4	8034.8701	10000	0.08968	0.02149	10044	1.0044E6	3.383E-3	0.7	3.2	191.004	114.20	104.3
34.62	125.1	0.2767	41.004	22.4	365.4	8121.2202	10000	0.08968	0.02334	10152	1.0152E6	3.383E-3	0.7	3.2	192.004	106.20	100.1
30.78	116.8	0.2636	42.012	22.4	374.5	8251.7100	10000	0.09191	0.02747	10315	1.0315E6	3.383E-3	0.7	3.2	193.012	94.447	93.41
28.56	111.5	0.2561	42.988	22.4	372.0	8326.2998	10000	0.09130	0.02992	10408	1.0408E6	3.383E-3	0.7	3.2	193.988	87.606	89.20
26.29	106.2	0.2476	44.020	22.4	370.3	8400.8203	10000	0.09090	0.03284	10501	1.0501E6	3.383E-3	0.7	3.3	195.020	80.662	84.96
24.46	100.6	0.2431	45.008	22.4	386.9	8475.2500	10000	0.09495	0.03820	10594	1.0594E6	3.383E-3	0.8	3.3	196.008	75.040	80.51
21.10	92.43	0.2283	46.004	22.4	379.4	8574.4404	10000	0.09313	0.04441	10718	1.0718E6	3.384E-3	0.8	3.3	197.004	64.729	73.94
19.18	87.09	0.2203	46.988	22.4	406.7	8636.3701	10000	0.09982	0.05363	10795	1.0795E6	3.383E-3	0.8	3.3	197.988	58.858	69.67
16.92	81.41	0.2078	47.996	22.4	400.1	8698.5195	10000	0.09820	0.06037	10873	1.0873E6	3.383E-3	0.8	3.3	198.996	51.911	65.13
14.19	73.05	0.1943	49.008	22.4	391.8	8778.9004	10000	0.09617	0.07342	10974	1.0974E6	3.383E-3	0.8	3.3	200.008	43.540	58.44
12.31	67.62	0.1821	50.008	22.4	393.5	8828.0498	10000	0.09658	0.08606	11035	1.1035E6	3.384E-3	0.8	3.4	201.008	37.775	54.10
10.84	61.72	0.1755	51.008	22.4	388.5	8877.3398	10000	0.09536	0.1020	11097	1.1097E6	3.384E-3	0.9	3.4	202.008	33.242	49.38
9.232	55.66	0.1658	51.992	22.4	398.4	8920.0996	10000	0.09779	0.1286	11150	1.1150E6	3.383E-3	0.9	3.4	202.992	28.323	44.53
7.823	50.28	0.1556	53.004	22.4	395.1	8956.7402	10000	0.09698	0.1563	11196	1.1196E6	3.384E-3	0.9	3.4	204.004	24.000	40.23
6.274	44.29	0.1417	53.992	22.4	398.4	8993.3896	10000	0.09779	0.2031	11242	1.1242E6	3.384E-3	0.9	3.4	204.992	19.249	35.43
4.750	38.03	0.1249	54.992	22.4	389.4	9023.5098	10000	0.09556	0.2692	11279	1.1279E6	3.384E-3	0.9	3.4	205.992	14.574	30.42
3.586	32.71	0.1096	55.992	22.4	394.3	9047.8896	10000	0.09678	0.3684	11310	1.1310E6	3.383E-3	0.9	3.4	206.992	11.003	26.17
2.545	26.43	0.09629	56.992	22.4	415.8	9071.5303	10000	0.1021	0.5954	11339	1.1339E6	3.384E-3	0.9	3.5	207.992	7.8068	21.14
1.390	18.39	0.07561	58.144	22.4	399.3	9094.2803	10000	0.09800	1.181	11368	1.1368E6	3.384E-3	1.0	3.5	209.144	4.2650	14.71
0.9393	14.51	0.06474	59.008	22.4	413.3	9099.9697	10000	0.1014	1.964	11375	1.1375E6	3.384E-3	1.0	3.5	210.008	2.8818	11.61
0.3684	7.891	0.04669	60.020	22.4	414.2	9108.0498	10000	0.1016	6.651	11385	1.1385E6	3.384E-3	1.0	3.5	211.020	1.1302	6.313

